Deformation relief and grain boundary energy in the zone of local tetragonal-monoclinic transformation in yttria-stabilized zirconia
Kozlova T.V. 1, Sevostyanova I.N. 1, Shlyakhova G.V. 1, Buyakova S.P. 1
1Institute of Strength Physics and Materials Science of Siberian Branch of Russian Academy of Sciences, Tomsk, Russia
Email: kozlovatv@ispms.ru, sevir@ispms.ru, shgv@ispms.ru, sbuyakova@ispms.ru

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Atomic force microscopy was used to study the local tetragonal-monoclinic transformation under load in yttria-stabilized zirconia with different grain sizes near the Vickers indentation crack propagation zone. It was shown that an increase of the sintering temperature and holding time leads to a decrease in the grain boundary energy. The local tetragonal-monoclinic transformation and the formation of self-accommodating variant pairs of the martensite type lead to a decrease in the grain boundary energy and stress relaxation. Keywords: yttria stabilized zirconia (Y-TZP), atomic force microscopy, tetragonal-monoclinic transformation under load, grain boundary energy.
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