Detonation synthesis of metal nanoparticles and study of their morphology
Khlebanovsky N.A.1,2, Moroz B.L.1, Kashkarov A.O.2, Ten K.A.2, Lukyanov Ya.L.2, Gerasimov E.Yu.3, Sharafutdinov M.R.4
1Novosibirsk State University, Novosibirsk, Russia
2Lavrentyev Institute of Hydrodynamics, Siberian Branch, Russian Academy of Sciences, Novosibirsk, Russia
3Boreskov Institute of Catalysis, Siberian Branch of RAS, Novosibirsk, Russia
4Institute of Solid State Chemistry and Mechanochemistry, Siberian Branch, Russian Academy of Sciences, Novosibirsk, Russia
Email: n.khlebanovskii@g.nsu.ru

PDF
The influence of the characteristics of explosive composites based on PETN and RDX containing Fe(II) oxalate and Cu(II) oxalate and acetate on the morphology of metal-containing nanoparticles formed as a result of detonation was studied using structural analysis methods. It was shown that the composition of the decomposition products of Fe(II) oxalate under explosion conditions is similar to the composition of the products of its thermal decomposition. In contrast, metallic copper and Cu(II) oxide, which are formed during their thermal decomposition, are absent among the decomposition products of Cu(II) oxalate and acetate. For charges containing an additive of Fe(II) oxalate, it was found that the charge density has a stronger effect on the average size of iron-containing nanoparticles and their size distribution than the mass fraction of the additive. Keywords: detonation products, detonation synthesis, nanoparticle morphology, metal nanoparticles.
  1. B.P. Tolochko, A.P. Tchernyshev, K.A. Ten, E.R. Pruuel, I.L. Zhogin, P.I. Zubkov, N.Z. Lyakhov, L.A. Lukyanchikov, M.A. Sheromov. Fizika metallov i metallovedenie (in Russian) 105, 2 (145) (2008) (in Russian)
  2. V.V. Osipov, V.V. Platonov, V.V. Lisenkov, K.I. Demidova, S.V. Zayats, M.P. Zykova. ZhTF, 93 (10), 1481 (2023) (in Russian). DOI: 10.61011/JTF.2023.10.56287.124-23
  3. G.Partizan, B.Z. Mansurov, B.S. Medyanova, A.B. Koshanova, B.A. Aliev. ZhTF, 86 (11), 86 (2016) (in Russian). DOI: 10.21883/jtf.2016.11.43819.1763
  4. A.I. Sidorov, U.V. Yurina, O.A. Podsvirov. ZhTF 89 (7), 1079 (2019) (in Russian). DOI: 10.21883/JTF.2019.07.47803.2-19
  5. A.I. Ancharov, B.B. Bokhonov, P.I. Zubkov, P.I. Ivanov, A.M. Kartashov, N.Z. Lyakhov, L.A. Lukyanchikov, L.A. Merzhievsky, V.G. Svikh, K.A. Ten, V.M. Titov, B.P. Tolochko, M.R. Sharafutdinov, M.A. Sheromov. XVIII Mezhdunarodnaya konferentsiya. Vozdeistvie intensivnykh potokov energii na veshchestvo. Sb. dokl. Fizika ekstremal'nykh sostoyaniy veshchestva (2003), s. 97-98 (in Russian)
  6. A.O. Kashkarov, E.R. Pruuel, K.A. Ten, E.Yu. Gerasimov, S.I. Kremenko, I.A. Rubtsov, G.R. Dashapilov, P.A. Pyrjaev, B.L. Moroz. J. Phys.: Conf. Ser., 1147, 012037 (2019)
  7. L.A. Lukyanchikpv, L.A. Merzhievsky, O.V. Evdokov, P.I. Zubkov, N.Z. Lyakhov, E.R. Pruuel, K.A. Ten, B.P. Tolochko, M.R. Sharafutdinov. Ultradispersnye poroshki, nanostruktury, materialy: poluchenie. Svoistva primenenie. IV Staverovskie chteniya. Tr.Vserossiiskoy nauchno-tekhnicheskoy konf., Krasnoyarsk. 2006, s. 74 (in Russian)
  8. Yi Lu, Zhenping Zhu, Zhenyu Liu. Carbon, 43 (2), 2005
  9. H. Yan, T. Zhao, X. Li. Combust Explos Shock Waves, 51, 495 (2005). DOI: 10.1134/S0010508215040152
  10. Ning Luo, Xiaojie Li, Yuling Sun, Xiaohong Wang. J. Alloys Compounds, 505 (1), 352 (2010). DOI: 10.1016/j.jallcom.2010.05.181
  11. A.V. Tchurikov, I.A. Leenson. Elektrokhim. energetika, 11, 14 (2012) (in Russian)
  12. D.A. Pivovarov, Yu.Yu. Golubchikova, A.P. Ilyin. Izvestiya Tomskogo politekh. un-ta, 321 (3), 11 (2012) (in Russian)
  13. Zh. Lin, D. Han, Sh. Li. J. Thermal Analysis Calorimetry, 107, 471 (2012)
  14. S.B. Sibocoza, M.J. Moloto, F. Mtunzi, N. Moloto. Asian J. Chem., 34, 239 (2022)
  15. A.O. Kashkarov, E.R. Pruuel, K.A. Ten, E.Yu. Gerasimov, S.I. Kremenko, I.A. Rubtsov, G.R. Dashapilov, P.A. Pyrjaev, B.L. Moroz. J. Phys.: Conf. Series, 1147 (1), 012037 (2019). DOI: 10.1088/1742-6596/1147/1/012037
  16. A.P. Ershov, A.L. Kupershtokh. Fizika goreniya i vzryva, 3, 118 (1986) (in Russian)
  17. L.A. Feigin, D.I. Svergun, G.W. Taylor. Structure Analysis by Small-Angle X-Ray and Neutron Scattering (Plenum Press, NY., 1987), 335 p
  18. Vychislenie parametrov detonatsii Tchepmena-Zhuge energeticheskikh materialov Electronic source. Available at: https://ancient.hydro.nsc.ru/chem/gase_deton_ ref.php

Подсчитывается количество просмотров абстрактов ("html" на диаграммах) и полных версий статей ("pdf"). Просмотры с одинаковых IP-адресов засчитываются, если происходят с интервалом не менее 2-х часов.

Дата начала обработки статистических данных - 27 января 2016 г.

Publisher:

Ioffe Institute

Institute Officers:

Director: Sergei V. Ivanov

Contact us:

26 Polytekhnicheskaya, Saint Petersburg 194021, Russian Federation
Fax: +7 (812) 297 1017
Phone: +7 (812) 297 2245
E-mail: post@mail.ioffe.ru