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Electropulse (sparking") plasma sintering of fine-grained W + 10 %Ni tungsten alloys
Russian version
Е.А. Lantsev1, N.V. Malekhonova1, А.V. Nokhrin1, K.E. Smetanina1, A.A. Murashov1, A.V. Voronin1, Yu. V. Blagoveshchenskiy2, A.V. Terent’ev2
1Lobachevsky University of Nizhny Novgorod, Nizhny Novgorod, Russia
2Baikov Institute of Metallurgy and Materials Science, Russian Academy of Sciences, Moscow, Russia
Email: elancev@nifti.unn.ru, malekhonova@nifti.unn.ru, yuriblag@imet.ac.ru
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The paper has investigated mechanisms of solid-phase electropulse plasma sintering of the W + 10 weight%Ni tungsten pseudoalloy. The composite powders W nucleus- Ni shell" were produced by a chemical-metallurgical method of deposition of nickel from a salt solution to a surface of industrial submicron tungsten particles. In order to reduce the oxygen and oxides concentrations, the composite powders were annealed in hydrogen at the temperatures 400 oC-600 oC. It also included the X-ray studies of the phase composition, electron-microscopic studies of micro-structure parameters and measurement of hardness of the tungsten pseudoalloys. Using the Yang-Cutler model, diffusion mechanisms were defined, which determine kinetics of plasma sintering of the submicron powders W nucleus- Ni shell". It has been shown that energy of powder sintering activation corresponds to energy of activation of diffusion along the grain boundaries in nickel, whereas a key mechanism of powder compaction is Coble creep. Keywords: tungsten, electropulse plasma sintering, diffusion, hardness.
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