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Effect of mechanical activation on the internal structure and macroresponses of a lead-free multicomponent material based on alkali metal niobates
Russian version
Glazunova E. V. 1,2, Zorin D. I. 1, Andryushina I. N. 1, Shilkina l. A. 1, Nagaenko A. V. 3, Makarev D. I. 1, Verbenko I. A. 1, Reznichenko L. A. 1
1Southern Federal University, Research Institute of Physics, Rostov-on-Don, Russia
2Kh. Ibragimov Complex Institute of the Russian Academy of Sciences, Groznyi, Russia
3Southern Federal University, Institute of High Technology and Piezo Technic, Rostov-on-Don, Russia
Email: glazunova@sfedu.ru, dezorin@sfedu.ru, inandryushina@sfedu.ru, lashilkina@sfedu.ru, nagaenko@sfedu.ru, dimakaryev@sfedu.ru, iaverbenko@sfedu.ru, lareznichenko@sfedu.ru
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The paper reports on the patterns of influence of mechanically activating procedures on the internal structure (crystalline, grain) and electrophysical properties of compositions based on alkali metal niobates of the type (NaaKbLic)(NbdTamSbn)O3 with the participation of a combined modifier (Bi2O3+Fe2O3) and a non-isostructural compound CuNb2O6. It was determined, based on the results obtained, that the optimal conditions for the preparation of high-density, virtually impurity-free ceramics are mechanical activation for (10-15) min. It is evident that these technological conditions have the capacity to reduce dielectric losses and increase the values of macroresponses of the ceramics under investigation. Keywords: alkali metal niobates, technology, mechanical activation, internal structure, microstructure, macroresponses.
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