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Fabrication of Cu₂ZnSnSe₄ Thin Films by Selenising Cu_1.8Se, SnSe, and ZnSe Precursor Layers: Effects of the Sequence of Layers

Government of the Russia , programme 211, project No 02.A03.21.0006

FASO of Russia , АААА-А18-118020190112-8

Maskaeva L.N.^1,2, Markov V.F.^1,2, Gracheva E.A.¹, Voronin V.I.³, Kozhevnikova N.S.⁴, Martin R.W.⁵, Yakushev M.V.^1,3,4,5, Kuznetsov M.V.⁴

¹Ural Federal University, 19 Mira St., Ekaterinburg, Russia Ural Federal University, Ekaterinburg, Russia

²Ural Institute of State Fire Service, 22 Mira St., Ekaterinburg, Russia

Ural Institute of State Fire Service, Ekaterinburg, Russia

³Miheev Institute of Metal Physics of the Ural Branch Russian Academy of Sciences, 18 S. Kovalevskoy St.,, Ekaterinburg, Russia

Miheev Institute of Metal Physics of the Ural Branch Russian Academy of Sciences, Ekaterinburg, Russia

⁴Institute of Solid State Chemistry of the Ural Branch Russian Academy of Sciences, 91 Pervomaiskaya St., Ekaterinburg, Russia

Institute of Solid State Chemistry of the Ural Branch Russian Academy of Sciences, Ekaterinburg, Russia

⁵Department of Physics, SUPA, University of Strathclyde, 107 Rottenrow, G4 0NG Glasgow, UK

Department of Physics, SUPA, University of Strathclyde, Glasgow, UK

Email: larisamaskaeva@yandex.ru, v.f.markov@urfu.ru, ka_fed-ra@mail.ru, voronin@imp.uran.ru, kozhevnikova@ihim.uran.ru, r.w.martin@strath.ac.uk, michael.yakushev@strath.ac.uk, kuznetsov@ihim.uran.ru

Поступила в редакцию: 5 апреля 2021 г.

Выставление онлайн: 9 июня 2021 г.

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Thin films of Cu₂ZnSnSe₄ (CZTSe) with a deficiency of Cu and Zn excess are fabricated by a selenisation of precursors composed of several layers of the selenides Cu_1.8Se, SnSe, and ZnSe (with different sequences of the layers), deposited on glass substrates from water-based solutions. The elemental composition of the films is examined by electron dispersive analysis and X-ray photoelectron spectroscopy whereas the structure is analysed by X-ray diffraction. Films fabricated from precursors with the selenide layer sequence Cu_1.8Se|SnSe|ZnSe|SnSe demonstrate the CZTSe kesterite structure, whereas those produced from precursors with other sequences of the selenides are mixtures of binary phases. Keywords: CZTSe, chemical bath deposition, structure, thin films, absorber.

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Дата начала обработки статистических данных - 27 января 2016 г.

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